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Judgment of cooling capacity balance of distillation column in air separation plant

Judgment of cooling capacity balance of distillation column in air separation plant
Oct 15, 2024
Author: DEAR AST
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In order to ensure the stable operation of the distillation column, the in and out material and its state of the distillation column needs to meet the material balance, component balance and energy balance. The main cooling liquid oxygen surface is an important indicator of whether the cooling capacity of the air separation plant is balanced or not. When the cooling loss of the unit is greater than the cooling capacity, the moisture content of the air entering and leaving the column (the liquid content in the saturated air) will be reduced, and the nitrogen to be condensate in main cooling needs to be condensed, the evaporation of liquid oxygen will also increase, and the surface of liquid oxygen will decrease. On the contrary, when the cooling capacity is greater than the cooling loss of the unit, the moisture content of the air entering the lower column will increase, and the amount of nitrogen to be condensed in the main cooling system will decrease, and the liquid oxygen surface will naturally increase.

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When the amount of processing air is reduced, the rising steam and reflux liquid in the upper column will be reduced, but the reflux ratio will not change. Therefore, the reduction of processing air in a small range will not affect the purity of oxygen and nitrogen, and the reduction of processing air volume will help to reduce the pressure of the upper and lower columns. However, according to the material balance, the production of oxygen and nitrogen will naturally decrease when the amount of processing air is reduced. If the amount of processing air is too small, there will be leakage on the tray. If the heat and mass exchange of the leaked liquid is not sufficient, the purity of oxygen and nitrogen will be greatly affected, and even the normal production can not be realized. Therefore, the minimum allowable load of distillation column is generally specified.
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