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How to shorten the start-up time of the full low-voltage air separation plant in the self-cleaning process?

How to shorten the start-up time of the full low-voltage air separation plant in the self-cleaning process?
Aug 15, 2023
Author: DEAR AST
Question Reply

The heat capacity of Plate-fin switching heat exchanger is small,Air separation equipmentThe start time is short, at 30 ~ 36 H level; the start time of the air separation unit with stone cooler needs 48 ~ 60h.
In terms of operation, master the essentials of operation: prevent moisture and carbon dioxide from being brought into the tower; strictly control the temperature difference between the cold end and the hot end; pay attention to the cooling of the main cooling; give full play to the refrigeration capacity of multiple expansion machines; reasonable allocation and utilization of cooling capacity, depending on the potential of the equipment itself to shorten the start-up time.
Because of the large heat capacity of the stone cooler, it takes quite a long time to cool down to normal temperature after heating. The air of the turbine air compressor can be used to blow the stuffing to near normal temperature before starting the expansion machine, and hot air can be discharged from the automatic valve box. In this way, the precooling time of the stuffing can be shortened.
In addition, using external cold source is also an effective way to shorten the start-up time. When the main cooling is over and liquid appears, input liquid oxygen, liquid or liquid nitrogen from the outside. The method of infusion is to connect the liquid source with the liquid oxygen discharge valve, open the liquid oxygen discharge valve and inject the external liquid into the main cooling. When the main cold liquid level reaches the normal liquid level, the infusion can be stopped, and the air separation tower can enter the stage of purging. With this infusion technology, the start-up time can be shortened by more than 12 hours. This is a very economical method, which has been applied in many units and has achieved practical energy saving effect.
The source of the liquid can be provided by another running air separation plant; it can also be discharged into the storage tank for standby when parking; it can also be introduced from the low temperature storage tank of liquid oxygen.

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When the amount of processing air is reduced, the rising steam and reflux liquid in the upper column will be reduced, but the reflux ratio will not change. Therefore, the reduction of processing air in a small range will not affect the purity of oxygen and nitrogen, and the reduction of processing air volume will help to reduce the pressure of the upper and lower columns. However, according to the material balance, the production of oxygen and nitrogen will naturally decrease when the amount of processing air is reduced. If the amount of processing air is too small, there will be leakage on the tray. If the heat and mass exchange of the leaked liquid is not sufficient, the purity of oxygen and nitrogen will be greatly affected, and even the normal production can not be realized. Therefore, the minimum allowable load of distillation column is generally specified.
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