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What are the technical requirements of the distillation column under the air separation plant?

What are the technical requirements of the distillation column under the air separation plant?
Aug 14, 2023
Author: DEAR AST
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Answer: 1. The manufacture, inspection and acceptance of the lower distillation column comply with the provisions of JB/T2549-1994 "aluminum air separation equipment manufacturing technical specification" and JB/T4734-2002 "Aluminum Welding container.

2. the welding joints of Class A and B of containers should be tested 100% Ray to meet the second level requirements of JB/t4730-2005 non-destructive testing of pressure equipment; the welding joints of class C and D and those that cannot be detected by Ray should be 100% penetrated to meet the level I requirements of JB/t4730-2005.
3. after the container is manufactured and compounded with the main cold, use dry and clean air or nitrogen to 0. 69MPa conduct the barometric test on the surface pressure, keep the pressure for 30 min, and there should be no obvious deformation or leakage, and then reduce it to 0. 6MPa conduct the air tightness test under the pressure gauge, and keep the pressure Zh from leaking.
4. Test procedures refer to pressure vessel safety technology supervision regulations.
5. All parts must be oiled before assembly or after repair, and the cleanliness should meet the relevant requirements of JB/T 6869-1993 air separation equipment surface cleanliness.
6. The distance between the weld line of the tube and the plane of the tower plate is 90mm, and the strengthening nut should be riveted tightly after tightening to prevent loosening.

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When the amount of processing air is reduced, the rising steam and reflux liquid in the upper column will be reduced, but the reflux ratio will not change. Therefore, the reduction of processing air in a small range will not affect the purity of oxygen and nitrogen, and the reduction of processing air volume will help to reduce the pressure of the upper and lower columns. However, according to the material balance, the production of oxygen and nitrogen will naturally decrease when the amount of processing air is reduced. If the amount of processing air is too small, there will be leakage on the tray. If the heat and mass exchange of the leaked liquid is not sufficient, the purity of oxygen and nitrogen will be greatly affected, and even the normal production can not be realized. Therefore, the minimum allowable load of distillation column is generally specified.
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