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How to regulate the cooling capacity of an air separation unit?

How to regulate the cooling capacity of an air separation unit?
Dec 06, 2024
Author: DEAR AST

The regulation of the cooling capacity of the air separation unit is a complex and delicate process, involving several operational aspects and parameter adjustments.
Appropriate closing of the oxygen and nitrogen delivery valves can increase the low and medium pressure, thus reducing the cooling capacity. Turbine expander air inlet adjustment adjustable nozzle, the opening is small, the refrigeration capacity is reduced. If the main cooling liquid level increases, the yield and purity of the product gas oxygen, argon distillate in the oxygen content decreases, so that the distillation conditions deteriorate, then the expansion air volume should be reduced. Open the bottom of the heat exchanger blow-off valve, you can exclude some of the overcooled liquefied air, which helps to regulate the amount of cold. When there is liquid oxygen level in the main cooling, the throttle valve of the main tower startup line should be fully closed to regulate the cooling capacity. Proper control of the air compressor cooling water can increase the temperature of the high-pressure air into the tower, which affects the cooling capacity. During the cooling phase, the cooling capacity of the expander should be maximized. As the temperature in the tower decreases, the expansion volume should be gradually increased to regulate the working condition of the expander and maintain the maximum cooling capacity. Appropriate discharge of some liquid oxygen can consume part of the cooling capacity. However, it should be noted that the liquid oxygen level should not be lower than a certain value to avoid affecting the normal operation of the air separation unit.
In the process of adjusting the cooling capacity, it should be kept stable and avoid drastic fluctuation. Keep the pressure inside the air separation unit stable and avoid over-pressure or low-pressure operation. Closely monitor the purity of the product oxygen to ensure that it meets the production requirements.

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When the amount of processing air is reduced, the rising steam and reflux liquid in the upper column will be reduced, but the reflux ratio will not change. Therefore, the reduction of processing air in a small range will not affect the purity of oxygen and nitrogen, and the reduction of processing air volume will help to reduce the pressure of the upper and lower columns. However, according to the material balance, the production of oxygen and nitrogen will naturally decrease when the amount of processing air is reduced. If the amount of processing air is too small, there will be leakage on the tray. If the heat and mass exchange of the leaked liquid is not sufficient, the purity of oxygen and nitrogen will be greatly affected, and even the normal production can not be realized. Therefore, the minimum allowable load of distillation column is generally specified.
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