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Liquid nitrogen pressurization process

Liquid nitrogen pressurization process
Jun 06, 2024
Author: DEAR AST

The liquid oxygen from the main condensing evaporator is compressed by the internal compressed oxygen pump, evaporated and reheated, and then enters the main heat exchanger. The liquid oxygen then flows out of the cold box as an oxygen product. The low pressure nitrogen is pumped out of the top of the low pressure tower and its cooling capacity is transferred to the return liquid in the sub-cooler. The cooling capacity is sent out of the cold box via the main heat exchanger, part of which is compressed by the first stage charge nitrogen compressor and sent to the nitrogen recirculation compressor. A portion is sent out as a low pressure nitrogen product. The remainder is further compressed by the charge nitrogen compressor, cooled by the aftercooler and sent out as a low pressure nitrogen product.

The medium pressure nitrogen is fed out of the first section of the nitrogen recirculation compressor (after the intercooler). The high pressure nitrogen is delivered from the second stage of the nitrogen cycle compressor (before the intercooler). The ultra-high pressure nitrogen is delivered from the last section of the nitrogen cycle compressor (before the compressor aftercooler).

The liquid nitrogen product comes from the main condensing evaporator, where one stream of liquid nitrogen product is cooled in the cooler and flows out of the cold box to provide subcooled liquid nitrogen for the liquid nitrogen cleaning unit. The other stream of liquid nitrogen is fed directly into the storage tank. The instrument air and plant air products are extracted from the process air after the molecular sieve and further compressed to the required pressure by a single stage air compressor with an aftercooler.

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When the amount of processing air is reduced, the rising steam and reflux liquid in the upper column will be reduced, but the reflux ratio will not change. Therefore, the reduction of processing air in a small range will not affect the purity of oxygen and nitrogen, and the reduction of processing air volume will help to reduce the pressure of the upper and lower columns. However, according to the material balance, the production of oxygen and nitrogen will naturally decrease when the amount of processing air is reduced. If the amount of processing air is too small, there will be leakage on the tray. If the heat and mass exchange of the leaked liquid is not sufficient, the purity of oxygen and nitrogen will be greatly affected, and even the normal production can not be realized. Therefore, the minimum allowable load of distillation column is generally specified.
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