Large air separation FAQ

1. Before connecting the pipe orifice of each container, clean white cloth shall be used to tie the orifice to prevent grease and dirt from entering. 2. When welding in the cold box and in the condensing evaporator, it is strictly forbidden for flame or arc to touch the surface of vessels and pipes. 3. The containers, valves, pipes and corresponding supports in the cold box, the surface of the cold box and the foundation surface shall not be stained with grease after installation, otherwise, degreasing treatment shall be carried out.

Air cooling column is a mixed heat exchange device. The function is to make the cooling water fully contact with the air and being mixed fully to increase the heat transfer area and enhance the heat transfer, usually using "packed column" or "sieve plate". The packed column is a round steel container with packing (ceramic ring, plastic ring, etc.). Cooling water is ejected from the top of the column and mixed with air flowing upward from the bottom for heat and mass exchange. Air transfers heat to the cooling water, lowering its temperature and raising its temperature. In order to prevent the generation of water droplets in the air, the raschig ring (or stainless steel wire mesh) packing separator (also known as trapping layer) and mechanical water separator (inertial separation) are usually installed on the upper part of the column. The cooling water ejected from the spray device flows downward to the packing layer through the distributor, and an overflow ring is provided to redist

All low pressure air separation units are usually equipped with nitrogen water precoolers. It mainly uses the unsaturation of nitrogen in sewage to evaporate part of water. As the water evaporates, it absorbs the latent heat of vaporization to lower the temperature of the cooling water, which is then used to cool the treated air and lower the temperature of the air entering the column. Therefore, it includes air cooling column and water cooling column. The basic purpose of setting up nitrogen precooler is to reduce the air temperature entering the air separation column and avoid the temperature fluctuation greatly. Because the inlet air temperature directly affects the operation conditions of the switching heat ex-changer and distillation column, as well as the economy of the whole air separation unit. In the design, the air temperature entering the column is usually set at 30 ° C. When the inlet temperature of the column is higher than the design index during operation, the throttl

The amount of liquid nitrogen removed from the lower column of the air separation unit will affect the purity of the liquid nitrogen in the lower column and the oxygen enriched liquid air at the bottom of the column. When the liquid nitrogen removal amount of the lower column increases, the reflux liquid participating in the heat and mass exchange of the lower column will be reduced, the temperature rise of the rising steam on the column plate will be correspondingly reduced, the condensation of the rising steam will not be sufficient, the oxygen component will be condensed less, the purity of nitrogen at the column top will be reduced, and the purity of liquid nitrogen will be naturally reduced. At the same time, the temperature rise of the downflow liquid will increase, the liquid evaporation will be more sufficient, more nitrogen components will be evaporated to the top of the column, and the purity of the liquid air at the bottom of the column will be improved accordingly.

Lean alloy steel is often used in special pressure-bearing equipment. The alloying elements often added include manganese, silicon, chromium, nickel, molybdenum, vanadium, boron and rare earth elements. Most of silicon and manganese melt into ferrite, only a small amount into cementite, which are commonly used strengthening elements in lean alloy steel. The amount of chromium and nickel is generally small, and the main role of chromium and nickel is to increase the undercooling degree of austenite and refine the microstructure. Part of chromium is dissolved in ferrite and some in cementite, which can improve the stability of cementite. Molybdenum is dissolved in ferrite slightly, and has the effect of solid solution strengthening. It is a strong carbide forming element, which can improve the high temperature strength of steel and improve the temper brittleness.

After a long-term operation of the air separation plant, the components in the cryogenic equipment and pipelines in the distillation system will be blocked due to ice or mechanical powder, which will increase the resistance of the fractionator. When the air separation plant has been in normal operation for about 2 years, the fractionator system should be heated and thawed to remove these deposits. When the molecular sieve adsorber and the main heat exchanger have water inflow or other faults, it is also necessary to stop and heat up. In general, the following methods will be used for heating and thawing.

After a long-term operation of the air separation plant, the components in the low-temperature equipment and pipelines of the distillation system will be blocked due to the internal precipitation of icing or mechanical powder, which will increase the resistance of the fractionating column. Therefore, after the normal operation of the air separation plant for about 2 years, the fractionating column system should be heated and thawed to remove these sediments. When the molecular sieve adsorber and the main heat exchanger have water or other faults, they must also be stopped for heating. The following describes several heating and thawing operation methods: